Intramolecular Cyclisation of Phenolic Oximes, III.A Synthesis ofcis‐cis‐Aerothionin
作者:
Alexander R. Forrester,
Ronald H. Thomson,
Soo‐On Woo,
期刊:
Justus Liebigs Annalen der Chemie
(WILEY Available online 1978)
卷期:
Volume 1978,
issue 1
页码: 66-73
ISSN:0075-4617
年代: 1978
DOI:10.1002/jlac.197819780108
出版商: WILEY‐VCH Verlag
数据来源: WILEY
摘要:
AbstractCis‐cis‐aerothionin has been synthesised by oxidative cyclisation of the diphenolic dioxime4with 2,4,4,6‐tetrabromocyclohexa‐2,5‐dienone followed by reduction with sodium tetrahydroborate. Certain methyl ethers react with cold pyridine giving misleading results when this solvent is used for1H‐NMR s
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