Preparation of 4‐pyrimidinetliiones from acyl lsothiocyanate‐enamine adducts
作者:
Robert W. Lamon,
期刊:
Journal of Heterocyclic Chemistry
(WILEY Available online 1969)
卷期:
Volume 6,
issue 1
页码: 37-41
ISSN:0022-152X
年代: 1969
DOI:10.1002/jhet.5570060107
出版商: Wiley‐Blackwell
数据来源: WILEY
摘要:
AbstractAdducts formed from benzoyl isothiocyanate and l‐morpholinocyclopentene or β‐(N,N‐diethylamino)styrene and that prepared from acetyl isothiocyanate and l‐pyrrolidinoeyclopen‐tene gave 4‐pyrimidinethiones when treated with primary amines or ammonia. In some cases intermediates, the products of amine exchange, were isolated. These intermediates were readily cyclized to 4‐pyrimidinethiones with
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