A low‐temperature apparatus for single‐crystal diffractometry. The unit‐cell dimension of α‐quartz in the temperature range 86–298 K
作者:
S. Danielsson,
I. Grenthe,
Å. Oskarsson,
期刊:
Journal of Applied Crystallography
(WILEY Available online 1976)
卷期:
Volume 9,
issue 1
页码: 14-17
ISSN:1600-5767
年代: 1976
DOI:10.1107/S0021889876010418
出版商: International Union of Crystallography
数据来源: WILEY
摘要:
A detailed description of an automatic low‐temperature apparatus to be used in single‐crystal diffractometry is given. The crystal is cooled by a stream of nitrogen gas. Prevention of ice formation on the crystal is achieved by heating the outer parts of the gas stream by a conical metal device. The unit‐cell dimensions of α‐quartz have been determined in the temperature range 86–298 K with this apparatus on a four‐circle diffractometer
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