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A low‐temperature apparatus for single‐crystal diffractometry. The unit‐cell dimension of α‐quartz in the temperature range 86–298 K

 

作者: S. Danielsson,   I. Grenthe,   Å. Oskarsson,  

 

期刊: Journal of Applied Crystallography  (WILEY Available online 1976)
卷期: Volume 9, issue 1  

页码: 14-17

 

ISSN:1600-5767

 

年代: 1976

 

DOI:10.1107/S0021889876010418

 

出版商: International Union of Crystallography

 

数据来源: WILEY

 

摘要:

A detailed description of an automatic low‐temperature apparatus to be used in single‐crystal diffractometry is given. The crystal is cooled by a stream of nitrogen gas. Prevention of ice formation on the crystal is achieved by heating the outer parts of the gas stream by a conical metal device. The unit‐cell dimensions of α‐quartz have been determined in the temperature range 86–298 K with this apparatus on a four‐circle diffractometer

 

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