Preparation of [1‐13C], [3‐13C], [1‐D]and [3‐D] Enriched Cyclobutenes
作者:
Børge Bak,
Jens Jørgen Led,
期刊:
Journal of Labelled Compounds
(WILEY Available online 1968)
卷期:
Volume 4,
issue 1
页码: 22-27
ISSN:0022-2135
年代: 1968
DOI:10.1002/jlcr.2590040105
出版商: John Wiley&Sons, Ltd.
数据来源: WILEY
摘要:
AbstractThree isotopically enriched samples of cyclobutene have been prepared, namely, a mixture containing 20 % [1‐13C]cyclobutene, 20 % [3‐13C]cyclobutene and 60 % parent molecule; a second mixture of 75 % [1‐D]cyclobutene and 25 % parent molecule; and a third mixture of 50 % [3‐D]cyclobutene and 50 % parent molecule. Proton magnetic resonance and infrared spectra showed the samples to be of high purity (>95 %). The preparations successfully have been used for high‐resolution microwave studies. The observed microwave line intensities also agreed with the percentage compositions gi
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