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Preparation of [1‐13C], [3‐13C], [1‐D]and [3‐D] Enriched Cyclobutenes

 

作者: Børge Bak,   Jens Jørgen Led,  

 

期刊: Journal of Labelled Compounds  (WILEY Available online 1968)
卷期: Volume 4, issue 1  

页码: 22-27

 

ISSN:0022-2135

 

年代: 1968

 

DOI:10.1002/jlcr.2590040105

 

出版商: John Wiley&Sons, Ltd.

 

数据来源: WILEY

 

摘要:

AbstractThree isotopically enriched samples of cyclobutene have been prepared, namely, a mixture containing 20 % [1‐13C]cyclobutene, 20 % [3‐13C]cyclobutene and 60 % parent molecule; a second mixture of 75 % [1‐D]cyclobutene and 25 % parent molecule; and a third mixture of 50 % [3‐D]cyclobutene and 50 % parent molecule. Proton magnetic resonance and infrared spectra showed the samples to be of high purity (>95 %). The preparations successfully have been used for high‐resolution microwave studies. The observed microwave line intensities also agreed with the percentage compositions gi

 

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