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Conversion of A‐60 NMR spectrometers to Fourier transform operation

 

作者: M. Tomkiewicz,   W. J. Horsley,   M. P. Klein,  

 

期刊: Review of Scientific Instruments  (AIP Available online 1975)
卷期: Volume 46, issue 8  

页码: 1112-1115

 

ISSN:0034-6748

 

年代: 1975

 

DOI:10.1063/1.1134361

 

出版商: AIP

 

数据来源: AIP

 

摘要:

A description of the instrumental modifications and additions required for the conversion of this class of field‐swept, field‐modulated 60‐MHz NMR spectrometers is given. The rf portions are straightforward adaptations of the single‐coil sample circuit to pulsed operation. The standard instrument achieves field‐frequency stabilization through use of a NMR sideband oscillator employing a separate sample. While such a configuration is adequate for the normal mode of operation, it does not provide sufficient absolute stability for the pulsed Fourier mode of operation. The requisite stability was achieved by phase locking the sideband oscillation frequency to an external reference by forcing the radio frequency to change in accordance with the phase‐lock error signal. Both analytical and control channels are driven by this common rf source, as is the reference signal to the analytical channel synchronous detector.

 

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