A Ceramic Sample Heater for Variable Temperature Diffuse Reflectance Fourier Transform Infrared Spectroscopy
作者:
R Lin,
RL. White,
期刊:
Instrumentation Science & Technology
(Taylor Available online 1996)
卷期:
Volume 24,
issue 1
页码: 37-45
ISSN:1073-9149
年代: 1996
DOI:10.1080/10739149608000464
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
A combination sample holder/heater that can be used for variable temperature infrared spectroscopic studies of solids is described. The ceramic sample holder/heater is durable and can be used to heat samples to temperatures as high as 1000 C under vacuum or in inert, reductive, or oxidative atmospheres. The design and properties of the ceramic heater are described and compared to those for a stainless steel sample holder containing a cartridge heater. Results from variable temperature infrared analysis of a sulfated zirconia solid acid catalyst obtained by using the ceramic heater are presented to illustrate the advantages of this sample holder/heater design.
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