On Line Extraction and Separation of Bendiocarb, Methomyl, Methylparathion, and Pentachlorophenol Pesticides from Raw Milk
作者:
M.L. Menezes,
G. Fèlix,
期刊:
Journal of Liquid Chromatography & Related Technologies
(Taylor Available online 1998)
卷期:
Volume 21,
issue 18
页码: 2863-2871
ISSN:1082-6076
年代: 1998
DOI:10.1080/10826079808003449
出版商: Taylor & Francis Group
数据来源: Taylor
摘要:
A high performance liquid chromatography (HPLC) method for extraction and determination of pesticides from raw milk was developed. The method involves direct injection of raw milk samples on a bovine serum albumin-dimethyl-octyl-silica gel (BSA-Si-C8) column. The mobile phase 0.05 mol.L−1phosphate buffer pH6.0 in acetonitrile (70:30 v/v) was employed for extraction and separation of bendiocarb, methylparathion, pentachlorophenol, and methomyl pesticides. The method shows good results of recovery in the pesticides studied, higher than 99.6%.
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