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Mass Spectral Studies of Biheteroaryls: Part 3. Identification of Dimeric Products Obtained from the Homolytic Methylation of the Lutidines

 

作者: KennethC. Bass,   Barry McIntosh,   AlanG. Osborne,  

 

期刊: Spectroscopy Letters  （Taylor Available online 1985）
卷期: Volume 18, issue 1  

页码: 35-46

 

ISSN:0038-7010

 

年代: 1985

 

DOI:10.1080/00387018509438133

 

出版商: Taylor & Francis Group

 

关键词: Gas chromatography — mass spectrometry;hemolytic methylation;dipyridylethanes;fragmentation

 

数据来源: Taylor

 

摘要:

The dimeric products formed during the homolytic methylation of the lutidines witht-butyl peroxide at 135° have been identified by gas chromatography — mass spectrometry. The 2,6- and 3,5- lutidines gave the corresponding dimethyldipyridylethanes whilst the 2,4-, 2,5- and 3,4- lutidines gave both the normal and crossed products.

 

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