Automatic collection of powder data from photographs
作者:
E. J. Sonneveld,
J. W. Visser,
期刊:
Journal of Applied Crystallography
(WILEY Available online 1975)
卷期:
Volume 8,
issue 1
页码: 1-7
ISSN:1600-5767
年代: 1975
DOI:10.1107/S0021889875009417
出版商: International Union of Crystallography
数据来源: WILEY
摘要:
A method is presented of determining powder data from photographs. With a microphotometer the density is measured in steps of 0.01° 2θ. These data are used by a computer program. With this program the background and the noise level are determined first. After the detection of the diffraction peaks, the peak positions and intensities are refined, a suitable model for the peak profile being used. A procedure is described for scaling of several photographs. The final results are illustrated with a comparison of 2θ values determined according to this method and the calculated values of the lattice refined with these data. The resulting data prove to be equivalent to the data obtained by conventional means. The computer program is written in FORTRAN
点击下载:
PDF
(960KB)
返 回