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Oxygen-17 NMR Spectra of Some Group VIB and VIIB Transition Metal Chalcarbonyl Complexes

 

作者: JamesP. Hickey,   IoneM. Baibich,   IanS. Butler,   LeeJ. Todd,  

 

期刊: Spectroscopy Letters  （Taylor Available online 1978）
卷期: Volume 11, issue 9  

页码: 671-680

 

ISSN:0038-7010

 

年代: 1978

 

DOI:10.1080/00387017808063439

 

出版商: Taylor & Francis Group

 

关键词: oxygen-17 nmr;transition metals;metal carbonyls;metal thiocarbonyls;metal selenocarbonyls;metal chalcocarbonyls;chromium;molybdenum;tungsten;manganese

 

数据来源: Taylor

 

摘要:

Although there are numerous reports in the literature on the13C nmr spectra of transition metal carbonyls,1little attention has thus far been focused on their17O nmr spectra.2-4Oxygen-17 nmr spectra are extremely difficult to obtain because of the quadrupolar nature of the17O nucleus (I = 5/2) and its low natural abundance (0.037%). In addition, the low

 

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