摘要:

Vllth INTERNATIONAL SYMPOSIUM ON LUMINESCENCE SPECTROMETRYDETECTION TECHNIQUES AND APPLICATIONS IN CHROMATOGRAPHY ANDCAPILLARY ELECTROPHORESISIN BIOMEDICAL ANALYSIS -Universit6 de Nice (Sophia Anti polis), FranceApril 17-19, 1996Organized by the University of Ghent (Belgium) in collaboration withthe University of Nice, the University of Tokyo and the Complutense University of MadridThis symposium envisages to report on the current status and future developments in the field ofluminescence techniques (fluorescence, chemiluminescence, electroluminescence, bioluminescence,phosphorescence and combinations with chromatography, capillary electrophoresis or immuno-assays) usedin drug quality control, clinical, chemical, biochemical, pharmaceutical, toxicological, food, environmentalanalyses and related areas.Original research papers can be submitted by registered participants to be presented in a general postersession; upon invitation, oral presentation may be suggested.Scientific CommitteeA.Alsina, SpainA.C. Calokerinos, GreeceB.J. Clark, EnglandJ. Crommen, BelgiumA. De Leenheer, BelgiumN. J. Dovichi, CanadaR. Fellous, FranceR.S. Givens, USAC. Gooijer, The NetherlandsG. Gubitz, AustriaN.A. Guzman, USAR. Haugland, USAH.T. Karnes, USAJ.R. Lakowicz, USAD. Lerner, FranceJ.N. Miller, EnglandK. Nakashima, JapanT.A. Nieman, USAOrganizing CommitteeW.R.G. Baeyens (Chairman), BelgiumD. De Keukeleire, BelgiumM. Rouillard, FranceK. Imai, JapanB. Del Castillo, SpainLocal Organizing CommitteeG.Van Der Weken, BelgiumC. Rawoens (Secretary) , BelgiumL. Liuani-Cuvelier, FranceA. Van Overbeke, Belgiuminvited SpeakersH. Lingeman, The NetherlandsD.L. Massart, BelgiumJ.-J. Aaron, FranceW. Adam, GermanyJ. J. Santana Rodriguez,A. Sanz Medel, SpainS.G. Schulman, USAH.H. Tannesen, NorwayA. Townshend, EnglandC. Van Peteghem, BelgiumT. Vo-Dinh, USAX. Xhang, ChinaSpainG. Rao, USAA. Rieutord, Fran ePublication: Proceedings of the conference will be published in The Analyst subject to the usual refereeingprocedures. Authors should send three copies of the manuscript to the Managing Editor, The Ana/yst, TheRoyal Society of Chemistry, at the address given in this journal, before the meeting or, at the latest, at themeeting, so that the paper can be processed rapidly.The manuscript should be in accordance with theInformation for Authors for The Analyst.The proceedings of the conference may be ordered directly from The Royal Society of Chemistry. Orderforms for this purpose will be made available at the meeting.Abstracts will be disseminated separately.Information: Professor Willy R.G. BAEYENS, Symposium Chairman, University of Ghent, PharmaceuticalInstitute, Department of Pharmaceutical Analysis, Laboratory of Drug Quality Control, Harelbekestraat 72,8-9000 Ghent (Belgium). Fax: +32 9 221 4175; Tel: +32 9 221 8951; E-mail: willy.baeyens@rug.ac.bAIRMON '96Second International Symposium on Modern Principles of Air Monitoring5-8 February 1996Salens Hogfjallshotell, Salen, SwedenThere is an increasing requirement for air monitoring within the preventive' framework of identifying andcontrolling health hazards at the workplace and in the environment.For the characterization of exposureto chemical and biological agents, sensitive, selective and user-friendly methods are needed. In recentyears there has been a rapid development in the area of air monitoring, and it is essential to promote theknowledge of newly developed mehtods for workplace, indoor and ambient air monitoring.*Target GroupAIRMON '96 is intended not only for scientists in academic circles working in the field, but also forenvironmental and health professionals in industry and officials from governmental and regulatory agen-cies.ObjectivesThe goals of the symposium are to provide a forum at which recent progress in analytical air samplingmethodology can be discussed and to provide an opportunity for an interchange of ideas among re-searchers, policy makers and practitioners in occupational health and environmental sciences.Regulatoryissues will also be addressed. After the symposium the participants will have a comprehen5ive knowledgeof recent developments in analytical measurement methodologyMAIN TOPICSSampling strategy - standardization - quality assurancePumped and diffusive sampling of organic compounds and inorganic gasesSampling of inorganic, organic and biological particulatesSampling of mixed phasesOrganizersAIRMON '96 is organized by the Nordic Institute for Advanced Training in Occupational Health(NIVA), the National Institute of Occupational Health, UmeA, Sweden and the National Institute ofOccupatioal Health, Oslo, Norway.NIVA is one of the institutes of the Nordic Council of Ministers and is located in Helsinki, Finland.Organizing CommitteeJan Olof Levin, NIOH, UmeA, ChairmanSiri Hetland, NIOH, OsloKurt Andersson, NIOH, UmeAMargaret Rhh, NIOH, UmeAYngvar Thomassen, NIOH, OsloADDRESSNational Institute of Occupational Health, P.O. Box 7654, S-907 UmeA, SwedenTel: 4 6 90 165066; Fax: +46 90 165027E-mail:margaretha.karlsson @nioh.s

ISSN:0003-2654    

DOI:10.1039/AN99520BP051

出版商:RSC    

年代:1995

数据来源: RSC

ISSN:0003-2654    

DOI:10.1039/AN99520FX054

出版商:RSC    

年代:1995

数据来源: RSC

摘要:

2888 Analyst, December 1995, Vol. 120 Xu, Xu-Qin, 1699 Xuejing, Xie, 1497 Yadav, R. B., 1099 Yamaguchi, Masatoshi, 1083 Yamamoto, Atsushi, 377, 1 137 Yaman, Mehmet, 101 Yaiiez-Lim6n. M., 1953 Yang, Jing-He, 2413 Yang, Jinghe, 1705 Yang, M. H., 1681 Yang, Yu, 243 Yao, Shouzhuo, 1885,2573,2833 Yau, Kei Wang, 1963 Yellig, Thomas J., 2775 Yermolaeva, T. N., 2387 Yilmaz, Selma, 1087 Yin, Wei, 2805 Yokota, Fumiaki, 2823 Young, Paul B., 2199 Yu, Ru-Qin, 499,2259,2829 Yuan, Ruo, 1055 Yuchi, Akio, 167 Zachariadis, George A,, 1593 Zachilas, Loukas N., 21 15 Zachwieja, Zofia, 943 Zagrodzki, Pawei, 943 Zaichick, Vladimir Ye., 8 17 Zaki, M. T. M., 549 Zamarreiio, M. M. Delgado, 2489 Zambenedetti, Pamela, 2425 Zambonin, Car10 G., 2185 Zambonin, Pier G., 2731 Zamrazil, Vklav, 959 Zanetti, Alberto, 1309 Zanoni, Maria Valnice B., 505 Zaratin, Laura, 1937 Zatta, Paolo F., 2425 Zelaya-Angel, O., 1953 Zen, Jyh-Myng, 5 1 1 Zhang, Aimei, 1195 Zhang, Fan, 121, 1699 Zhang, Feng-jun, 1603 Zhang, Shufen, 1599 Zhang, X.R., 463 Zhang, Yu-Hui, 2513 Zhang, Zhujun, 453, 2585 Zhao, Guohu, 2081 Zheng, Guo-Dong, 499 Zhi, Zheng-liang, 201 3 Zhou, Ge Rong, 2237 Zhu, Yu-rui, 2853 Zhuang, Hui-sheng. 121 Zolotov, Yury A., 201 Zuber, Paul A., 2873 Zufiaurre, Raquel, 75 12888 Analyst, December 1995, Vol. 120 Xu, Xu-Qin, 1699 Xuejing, Xie, 1497 Yadav, R. B., 1099 Yamaguchi, Masatoshi, 1083 Yamamoto, Atsushi, 377, 1 137 Yaman, Mehmet, 101 Yaiiez-Lim6n. M., 1953 Yang, Jing-He, 2413 Yang, Jinghe, 1705 Yang, M. H., 1681 Yang, Yu, 243 Yao, Shouzhuo, 1885,2573,2833 Yau, Kei Wang, 1963 Yellig, Thomas J., 2775 Yermolaeva, T.N., 2387 Yilmaz, Selma, 1087 Yin, Wei, 2805 Yokota, Fumiaki, 2823 Young, Paul B., 2199 Yu, Ru-Qin, 499,2259,2829 Yuan, Ruo, 1055 Yuchi, Akio, 167 Zachariadis, George A,, 1593 Zachilas, Loukas N., 21 15 Zachwieja, Zofia, 943 Zagrodzki, Pawei, 943 Zaichick, Vladimir Ye., 8 17 Zaki, M. T. M., 549 Zamarreiio, M. M. Delgado, 2489 Zambenedetti, Pamela, 2425 Zambonin, Car10 G., 2185 Zambonin, Pier G., 2731 Zamrazil, Vklav, 959 Zanetti, Alberto, 1309 Zanoni, Maria Valnice B., 505 Zaratin, Laura, 1937 Zatta, Paolo F., 2425 Zelaya-Angel, O., 1953 Zen, Jyh-Myng, 5 1 1 Zhang, Aimei, 1195 Zhang, Fan, 121, 1699 Zhang, Feng-jun, 1603 Zhang, Shufen, 1599 Zhang, X. R., 463 Zhang, Yu-Hui, 2513 Zhang, Zhujun, 453, 2585 Zhao, Guohu, 2081 Zheng, Guo-Dong, 499 Zhi, Zheng-liang, 201 3 Zhou, Ge Rong, 2237 Zhu, Yu-rui, 2853 Zhuang, Hui-sheng.121 Zolotov, Yury A., 201 Zuber, Paul A., 2873 Zufiaurre, Raquel, 75 12888 Analyst, December 1995, Vol. 120 Xu, Xu-Qin, 1699 Xuejing, Xie, 1497 Yadav, R. B., 1099 Yamaguchi, Masatoshi, 1083 Yamamoto, Atsushi, 377, 1 137 Yaman, Mehmet, 101 Yaiiez-Lim6n. M., 1953 Yang, Jing-He, 2413 Yang, Jinghe, 1705 Yang, M. H., 1681 Yang, Yu, 243 Yao, Shouzhuo, 1885,2573,2833 Yau, Kei Wang, 1963 Yellig, Thomas J., 2775 Yermolaeva, T. N., 2387 Yilmaz, Selma, 1087 Yin, Wei, 2805 Yokota, Fumiaki, 2823 Young, Paul B., 2199 Yu, Ru-Qin, 499,2259,2829 Yuan, Ruo, 1055 Yuchi, Akio, 167 Zachariadis, George A,, 1593 Zachilas, Loukas N., 21 15 Zachwieja, Zofia, 943 Zagrodzki, Pawei, 943 Zaichick, Vladimir Ye., 8 17 Zaki, M.T. M., 549 Zamarreiio, M. M. Delgado, 2489 Zambenedetti, Pamela, 2425 Zambonin, Car10 G., 2185 Zambonin, Pier G., 2731 Zamrazil, Vklav, 959 Zanetti, Alberto, 1309 Zanoni, Maria Valnice B., 505 Zaratin, Laura, 1937 Zatta, Paolo F., 2425 Zelaya-Angel, O., 1953 Zen, Jyh-Myng, 5 1 1 Zhang, Aimei, 1195 Zhang, Fan, 121, 1699 Zhang, Feng-jun, 1603 Zhang, Shufen, 1599 Zhang, X. R., 463 Zhang, Yu-Hui, 2513 Zhang, Zhujun, 453, 2585 Zhao, Guohu, 2081 Zheng, Guo-Dong, 499 Zhi, Zheng-liang, 201 3 Zhou, Ge Rong, 2237 Zhu, Yu-rui, 2853 Zhuang, Hui-sheng. 121 Zolotov, Yury A., 201 Zuber, Paul A., 2873 Zufiaurre, Raquel, 75 12888 Analyst, December 1995, Vol. 120 Xu, Xu-Qin, 1699 Xuejing, Xie, 1497 Yadav, R. B., 1099 Yamaguchi, Masatoshi, 1083 Yamamoto, Atsushi, 377, 1 137 Yaman, Mehmet, 101 Yaiiez-Lim6n.M., 1953 Yang, Jing-He, 2413 Yang, Jinghe, 1705 Yang, M. H., 1681 Yang, Yu, 243 Yao, Shouzhuo, 1885,2573,2833 Yau, Kei Wang, 1963 Yellig, Thomas J., 2775 Yermolaeva, T. N., 2387 Yilmaz, Selma, 1087 Yin, Wei, 2805 Yokota, Fumiaki, 2823 Young, Paul B., 2199 Yu, Ru-Qin, 499,2259,2829 Yuan, Ruo, 1055 Yuchi, Akio, 167 Zachariadis, George A,, 1593 Zachilas, Loukas N., 21 15 Zachwieja, Zofia, 943 Zagrodzki, Pawei, 943 Zaichick, Vladimir Ye., 8 17 Zaki, M. T. M., 549 Zamarreiio, M. M. Delgado, 2489 Zambenedetti, Pamela, 2425 Zambonin, Car10 G., 2185 Zambonin, Pier G., 2731 Zamrazil, Vklav, 959 Zanetti, Alberto, 1309 Zanoni, Maria Valnice B., 505 Zaratin, Laura, 1937 Zatta, Paolo F., 2425 Zelaya-Angel, O., 1953 Zen, Jyh-Myng, 5 1 1 Zhang, Aimei, 1195 Zhang, Fan, 121, 1699 Zhang, Feng-jun, 1603 Zhang, Shufen, 1599 Zhang, X. R., 463 Zhang, Yu-Hui, 2513 Zhang, Zhujun, 453, 2585 Zhao, Guohu, 2081 Zheng, Guo-Dong, 499 Zhi, Zheng-liang, 201 3 Zhou, Ge Rong, 2237 Zhu, Yu-rui, 2853 Zhuang, Hui-sheng. 121 Zolotov, Yury A., 201 Zuber, Paul A., 2873 Zufiaurre, Raquel, 75 1

ISSN:0003-2654    

DOI:10.1039/AN995200X056

出版商:RSC    

年代:1995

数据来源: RSC

ISSN:0003-2654    

DOI:10.1039/AN99520BX060

出版商:RSC    

年代:1995

数据来源: RSC

摘要:

Analyst, L>ecemht.l- 1995, Vo1. 120 155N -- __ Book Reviews Carbohydrate Analysis: High-performance Liquid Chro- matography and Capillary Electrophoresis Edited by Ziad El Rassi. Journal of Chromatography Library, Volume 28, Pp. xix + 627. Elsevier Science. 1995. Price $242.75. ISBN 0-444-89981-2. This book has as its prime objective the provision of a comprehensive review of carbohydrate analysis by using high- performance liquid chromatography (HPLC) and high-perfor- amance capillary electrophoresis (HPCE). The editor has set about achieving this goal by enlisting the help of several contributors of international repute. The scope of the book includes discussions on the fundamental aspects of the various modes of HPLC and HPCE as applicable :o carbohydrate analysis, analytical and preparative separations, principles of detection and quantitative determination of carbohydrates by HPLC and HPCE, and the very important area of sample preparation.The book contains seventeen chapters which 2re arranged into three major sections. Part 1, entitled ’The Solute’, comprises chapter 1 , which comprehensively reviews the several sample preparation strategies employed for carbohy- drates prior to analysis by HPLC and HPCE. At the end of this chapter there are two very useful tables: the first gives commercial sources of reference and other compounds useful in carbohydrate analysis and the second contains data on com- panies listed in the first table. Chapters 2 to 9 form Part 2 of the book and this goes under the heading ‘Analytical and Pre- parative Separations ’.Interactive modes of chromatography based on non-specific interactions, e.g., reversed phase, hydro- phobic interaction, hydrophilic interaction and ion exchange are covered in chapters 2 to 5. Chapter 6 deals with biospecific interaction (affinity) in chromatography and capillary electro- phoresis and this is followed by a review of size-exclusion chromatography (a non-interactive mode) in chapter 7. A succinct review on the various aspects of preparative HPLC for the isolation of intact and pure carbohydrates and glycoco~iju- gates is given in chapter 9. The topic of HPCE is thoroughly dealt with in chapter 8, which is the longest contribution in the book. This chapter provides ( a ) an overview of the funda- mentals of capillary electrophoresis, (h) an in-depth treatment of the electrophoretic system that is useful for the separation of a wide variety of carbohydrate species and (c) a comprehensive review of HPCE methodologies and applications.This is a well written and illustrated contribution. The remaining ejght chapters (chapters 10 to 17) constitute Part 3 which is headed ‘The Detection’. This is a very important and relevant topic since, in general, carbohydrates lack chromophores or fluor- ophores in their structures causing difficulties in determining these species at low levels. These chapters cover in detail various direct and indirect methods that have been used for the sensitive detection of carbohydrates following separation by either HPLC or HPCE. The basic principles, advantages.limitations and applications of the particular detection tech- nique are discussed in each of the chapters. The detection techniques discussed include electrochemical (chapter 1 O), refractive index (chapter 1 1 ), rnass spectrometry (chapter 121, evaporative light scattering (chapter 13). chiroptical (chapter 14), pre- and post-column derivatization (chapter I5), post- column enzyme reactors (chapter 16), indirect UV and fluorescence detection, low wavelength UV and other miscella- neous modes of detection (chapter 17). Each contribution has been well organiLed and presented, making good use of figures. diagrams and tables. A useful feature found at the end of chapter 5 is a section listing and explaining the abbreviations used in that contribution. This proved very valuable when reading that chapter and it would have been a good idea to have had this feature as part of each contribution.Inevitably there are some overlaps in the informa- tion being discussed in several of the contributions but reference is frequently made to the other contributions, thereby minimiz- ing the amount of unnecessary duplication. The editor has done an excellent job in bringing the contributions together and has succeeded in achieving the objective of providing a compre- hensive review of carbohydrate analysis by HPLC and HPCE. This volume is a valuable addition to the renowned Journal of Chromatography Library series and should have a wide appeal. It contains a wealth of useful information for those employing HPLC and HPCE (both experienced and inexperienced users) as separation tools for carbohydrate analysis and other fields of organic analysi5. E ma ti McKcvw 1 I Shell Research Chester, UK Information Theory in Analytical Chemistry By Karel Eckschlager and Klaus Danzer.A Series of Monographs on Analytical Chemistry and Its Applica- tions: Volume 728. Series editor J. D. Winefordner. Pp. xv + 276. 1994. Price €54.00. ISBN 0-471-59507-1. This book is a sequel to ‘Information Theory as Applied to chemical Analysis’ (volume 53, K. Eckschlager and V. Stgpanek, 1979’). The difference in the titles indicates that now information theory is part of the structure of methods of investigation, based upon chemical, physical and mathematical principles, within which modern analytical chemistry exists.Information theory has found enough applications to be able to present a systematical approach, as is evident from this book. For each analytical field of interest, the accompanying theoret- ical methods are dealt with. There are chapters on identification of components; quantitative analysis; qualitative analysis; niulticomponent analysis: distribution analysis (this covers microanalysis; surface analysis and scanning methods); and structure analysis. The authors present practical applications. Therefore the book is very useful in the laboratory. As an example one can take chapter 5 (qualitative analysis) in which the presence of a known component is tested. Selectivity is required here, and that requires dimensional analysis such as elemental analysis; atomic emission: X-ray fluorescence; or atomic absorption. The information content of the analysis is the sum of the signals chosen (e.g..diverse emission lines of an element). This is reconstructed out of the (im)probability of each of the signals, taking into account the separate problem of interferences and interactions. As with all the other chapters in this book, some practical applications and a handy, comprehensive literature overview is provided. A separate chapter is devoted to multivariate analyses, like pattern recognition, and factorial data analysis, in which restricted selectivity and differences in sensitivity and limits of detection are discussed. The profits of the theoretical calculations in the analysis (besides a greater knowledge of the analysis) are the practical implications to work out the optimum analytical strategy for a given problem.This and quality assurance are presented in two general chapters. A point of criticism niay be that another important output, the calculation of the probability of false positive and false negative results, is n d taken into account. The closing chapter is concerned with the question of whether information theory can be considered as the theoretical base of analytical chemistry. The statement by many analytical156N Analyst, December 1995, Vol. 120 chemists that the physical and chemical bases of their measuring methods are arguments to consider analytical chemistry as a separate science (as already stated by Ostwald) is not convincing. The authors straddle with two arguments: based on the science of information and based on the plethora of physical and chemical specialisms.The authors, Eckschlager and Danzer, are professors in Prague and Jena, respectively, and leading scientists in the field of information theory. The book is a brilliant compilation of theoretical fundamental and practical applications of information theory in analytical chemistry, especially useful as a tool for optimizing chemical analysis. It is by far the best book in this field currently available. We hope that analytical chemists will apply the tools offered here in their own situation in order to answer ‘what is the certainty of what we are doing and how can we improve it? ’ Dr. G. Dijkstra W. G. de Ruig State Institute for Quality Control of Agricultural Products The Netherlands ELISA: Theory and Practice By John R.Crowther. Methods in Molecular Biology, Volume 42. Pp. xi + 224. Humana Press. 1995. Price $59.50. ISRN 0-89603-279-5. The book’s avowed objective is ‘to introduce the experimenter to the technology known as the Enzyme Linked Immunosorbent Assay’. In reality, the book appears to be a set of badly edited course notes put between a ring binder. ELISA exploits the exquisite specificity and avidity which an antibody has for an antigen (the analyte). The reaction is detected and amplified by a system which includes an enzyme; the catalysis of many molecules of substrate by one molecule of the enzyme provides the amplification factor. Nowhere in the book can I find a comparably succinct definition or, indeed, anything that one could use as a definition of ELISA.It is difficult to know who the book is written for. On page 2 it delves straight into the complexities of the immune system, assuming the reader knows what the reticuloendothelial system and Kupffer cells are. In total contrast, on page 107 it describes the relationships between a litre and a millilitre, and the factors required to convert grams to milligrams, etc. The book only refers to ELISA in medical diagnosis; the areas of food, environment and drug abuse, for instance, are not mentioned. There are many ambiguous and misleading comments and unexplained nomenclature. Such as page 3: ‘therefore, the serum of any mammal (vertebrate) contains a heterogeneous mixture of immunoglobulin molecules.’ Should we infer that mammal equals vertebrate or that only vertebrate mammals(!) are included in the statement? On page 24: ‘enzymes, hyaluronidase are factors which facilitate invasion of infectious agents.’ Is hyaluronidase not an enzyme? Again, page 35: what is the difference between ‘Ab’ and ‘AB’? On page 53: ‘The antibody may have been raised in a given species, e.g., rabbit.’ How else could it have been raised? One could go on to cite many more instances; and also to point out redundant words, non sequiturs, confusing syntax and bad style.Micropipettes are described as ‘instruments that deliver volumes of liquid’-so does a bucket. In the procedure on page 93 it states ‘Incubate at 37 “C; two steps later it says, ‘if incubation has to be made at room temperature .. .’. Chapter 4 is entitled ‘Theoretical Considerations’, but includes mostly practical matters. All the examples of ELISA variants are prefaced with a paragraph entitled ‘Learning Principles.’ They are not: they are either objectives or activities. One has the feeling that the author of the book has immense practical experience of ELISA which could be of great value to those needing to become acquainted with the technique. The practical examples are potentially useful, and there are information and tips which I have not seen in print elsewhere. It is a pity that the writing only serves to obscure their value. The problem seems to be that the book is derived from the notes for a practical course, but without the rigorous editing which is necessary to convert it into a readable volume.One must seriously question the role of the publisher in this, since $60 for such a volume represents poor value for money. J . C. Allen Manchester Science Park Ltd Manchester, UK Advances in Chromatography. Volume 35 Edited by Phyllis R. Brown and Eli Grushka. Pp. xviii + 426. Marcel Dekker. 1995. Price $165.00. ISBN 0-8247-9361-7. 1995 sees the thirtieth anniversary of this great publication. During this period it had been an invaluable companion to the chromatographer. In the introduction to the series in Volume 1 (published in 1965) Cal Giddings and his co-editor, Roy Keller, wrote ‘The explosive growth of chromatography has made it difficult for any single individual to maintain a coherent view of the field’s progress. Original papers, even in many specialized areas of chomatography, are so numerous to hinder digestion’.This statement is as true today as it was thirty years ago: however, at that time it referred mainly to gas chromatography, it was made more prophetic by the development of high- performance liquid chromatography (HPLC), as well as by developments of other types of separation such as field flow fractionation (FFF), supercritical fluid-chromatography (SFC) and extraction (SFE), and capillary electrophoresis (CE). It is this latter technique which occupies over 50% of Volume 35, with four sections covering: Optical detector, it became obvious very early on that the growth of CE was limited partly by the inadequate detection power provided by the standard HPLC detector.This chapter covers subsequent developments; CE coupled with mass spectrometry, the on-line coupling of CE with MS, injection techniques, modification of capillary conditions, use of buffers and finally a number of applications; optimization of parameters, basic theoretical concepts together with a conservation of experimental variables which influence separation parameters; pharmaceutical analysis by CE, various modes of CE followed by applications covering a wide range of pharmaceutical classes, followed by a comparison of CE with HPLC. The true value of Volume 35 of Advances in Chromatography, is not only in the topics addressed in the eight chapters but in the vast number of references which they contain. The other four sections are no less interesting: Chiral separations, the evolution of Pirkle-type chiral stationary phases together with examples of the production of enantio- enriched compounds; reversed phase ion-pair, retention mecha- nism followed by examples of different factors which affect retention; characterization of gasolines; compound class method and Piona methods followed by examples covering benzene, aromatics, olefins and oxygenates; error sources in peak size rations, this is often a neglected and under- investigated area of chromatography, with the introduction of totally automated, computer controlled chromatographs. This isAnalyst, December 1995, Vol.120 157N a chapter well worth the attention of the unwary. The chapter covers incomplete resoluton, use of peak heights and integration errors.The true value of Volume 35 of Advances in Chromato- graphy, as in all the previous volumes, is not only in the topics addressed in the eight chapters but in the vast number of references which they contain, (1061 in this edition). Another thoroughly recommend reference volume for the chromato- grapher. F. Bailey Cheshire, UK NMR Spectroscopy. Second Edition. Basic Principles, Concepts and Applications in Chemistry By Harald Gunther. Pp. xx + 582. Wiley. 1995. Price f24.95. ISBN 0-471-95201-X. would serve as a brief introduction to the interested reader. Topics such as chemical induced nuclear polorization and paramagnetic materials are also included. These I believe are of some considerable benefit. It is, however, rather strange to see the nuclear Overhauser effect included in what is called a selected experimental technique, as it is a fundamental phenomenon of NMR.It is perhaps one of the problems of NMR that it is a subject that is so rapidly changing that it is virtually impossible to write an up to date text book. This author has struggled valiantly to update what is a rather old text book, but really the subject has moved on so far that only a complete rewrite could have hoped to have succeeded. P. S . Belton Institute of Food Research Norwich, UK It is noteworthy that in the original German version (published in 1992) the title properly reflected the fact that the book concentrates almost entirely on proton and carbon- 13 NMR and indeed, it is really true to say that it is a book concerned about proton NMR with some addenda on carbon-13 NMR.It would have been useful for the prospective reader had those limitations been reflected in the title. On opening the book it is fairly obvious that it is a second edition of a fairly old book, rather than a rewrite. Most of the spectra shown are CW-NMR spectra and the modern student will in fact probably only ever see such spectra in text books. This ‘datedness’ appears throughout the book. There are lengthy discussions on continuous wave methods which really are now largely irrelevant and, at best, should have been confined to an appendix. Similarly, the discussion of experi- mental aspects of Pulse Fourier Transform spectroscopy has a rather outdated feel to it. Given these limitations, however, there are some strong points to the book.Giinther is rather good at explaining things. I particularly liked the chapter on two-dimensional methods which offered a limited, but easy to follow introduction, to what is conceptually a difficult subject. Students could well benefit from reading this chapter before going on to the more rigorous, but less easy to follow, accounts that already exist in the literature. Even in this chapter, however, I had some reserva- tions. Key two-dimensional methods such as NOESY and experiments based on Hartmann Hahn and related polarization transfer methods are left until a later chapter. It would have been a great deal more coherent had all this information been kept together. This author has struggled valiantly to update what is a rather old text book, but really the subject has moved on so far that only a complete rewrite could have hoped to have succeeded.In addition to covering what one might term the usual subject matter for a text book on proton NMR spectroscopy, there are two additional chapters. One is an extended chapter on the influence of dynamic effects on proton nuclear magnetic resonance. This is clearly something that is close to the author’s heart and whilst perhaps. the chapter is rather long for a general text book, for the more specialized reader it represents a good introduction. The second additional chapter is called ‘selected experimental techniques of nuclear magnetic resonance spec- troscopy’. This contains a whole range of short sections on a wide variety of experimental techniques. There is a very succinct and easy-to-read account of solid state NMR which Recent Advances in Oilfield Chemistry Edited by P.H. Ogden. Pp. ix + 331. Royal Society of Chemistry. 1994. Price f62.50. ISBN 0-85186-941-6. Oilfield chemicals represent a relatively small but nevertheless important sector of the chemical industry. Efficient economic exploitation of oil reserves with simultaneous minimization of environmental impact means that close attention must be paid to the mode of action and fate of chemicals used in oil winning. The range of materials employed in drilling muds is quite diverse: from ester-based fluids, cationic polymers and lig- nosulfonates to inorganics such as metal hydroxides and cements. The formation of inorganic and asphaltene scales requires the use of inhibitors; and souring (originating in hydrogen sulfide formation) must also be overcome.This book reports the proceedings of the ‘Fifth International Symposium on Chemistry in the Oil Industry’, organized by the Industrial Division of the Royal Society of Chemistry and held in Ambleside, Cumbria, UK in April 1994. It contains 23 papers by a total of 70 authors, both chemists and petroleum engineers, almost all from Europe. The development, mode of action, and especially the environmental influence of the materials used in oilfields are discussed in considerable depth; an overview by R. C. Minton is particularly useful in setting the scene, and the papers are nearly all written at a level which is comprehensible to the non- specialist. The book can be recommended to all who work in developing and applying oilfield chemicals. Inevitably, though, this is a book of somewhat peripheral interest to analytical chemists, although analysis has a crucial role in many of the papers: the use of Fourier transform IR spectroscopy in characterizing cements by T. L. Hughes et al.; of size exclusion chromatography in assaying low levels of polymeric scale inhibitors by C. T. Bedford et al.; and of gas chromatography in characterizing reactions of sulfur com- pounds in crudes (G. G. Hoffman et al.) are all of interest. The editor and the publishers are to be congratulated in achieving rapid publication; camera-ready presentation means, therefore, that the typefaces differ markedly, but the overall presentation is fairly uniform, with a research paper format and references at the end of each chapter. There is a comprehensive subject index. Keith D. Bartle University of Leeds Leeds, UK

ISSN:0003-2654    

DOI:10.1039/AN995200155N

出版商:RSC    

年代:1995

数据来源: RSC

摘要:

158N Anulyst, Decenzher 199.5, bbl. 120 Conference Diary Date Conference Location 1996 January 8-9 Strategies for Identification of Novel Targets San Diego, for Drug Discovery USA 8- I 3 1996 Winter Conference on Plasma Florida, Spectrometry USA 10-13 Environmental Science Triv andrum, India 20-23 8th Sanibel Conference on Mass Spectrometry Sanibel Island, 21-25 VIth Latin American Congress on Caracas, 21-25 HPCE '96 Orlando, USA C hrorna tography Venezuela USA 29--3 I Analysis of Peptides February Stockholm. Sweden 4-7 5-8 6-7 7-9 20-2 1 The Fifth International Congress on Trace Elements in Medicine and Biology: Therapeutic Uses of Trace Elements Meribei, France Second International Symposium on Modern Principles of Air Monitoring Sweden Sden, European Symposium on Formulation of Paris, Poorly Available Drugs for Oral France Administration Fourth International Symposium on Bruges, Hyphenated Techniques in Chromatography Belgium (HTC 4); Hyphenated Chromatographic Analy sers Inbio '96: Industrial Biocatalysis Manchester, UK March 3-8 47th Pittsburgh Conference on Analytical Chicago, Chemistry and Applied Spectroscopy USA 7-8 Second Annual Genetic Screening and San Francisco, Diagnosis of Human Diseases USA Contact Cambridge Healthtech Institute, 1037 Chestnut Street, Newton Upper Falls, MA 02164 USA Tel: + I 617 630 1300.Fax: + I hi7 630 1325 E-mail: chi@healthtech.com R. Barnes, Department of Chemistry, Lederle GRC Tower, IJniversity of Massachusettes, P.O. Box 34510, Amherst, MA 01003-4510, USA Tel: + I 413 545 2294. Fax: +1 413 545 4490 Dr.C. S. P. Iyer, Convener, ICES-96, Regional Research Laboratory (CSIR). Trivandrum-695 0 19, India ?'el: +91 471 77459. Fax: +91 471 75186 E-mail: t-rit@sirnetm.esnet.in ASMS, 1201 Don Diego Ave., Santa Fe, NM 87505 Tel: +1 505 989 4517. Fax: + I 505 989 1073 Irene Romero, Interep SA, P.O. Box 76343, Caracas 1070-A, Venezuela Shirley E. Schlessinger, Symposium Manager, HPCE '96, Suite 101 5 , 400 East Randolph Drive, Chicago, IE 60601, USA Tel: +1 312 527 2011. Swedish Academy of Pharmaceutical Sciences, 2nd Symposium on Analysis of Peptides, P.O. Box 1136, S-1 I 1 81 Stockholm, Sweden Arlette Alcaraz, Chrug HGpital A. Michallon, Biochimie C, BP 217, F-38043 Grcnoble Cedex 9, France Tel: +33 767 65484. Fax: +33 767 65664 Pir,jo Xrtiainen, NIVA, Topeliuksenkatu 4 1 aA, FIN-00250 Helsinki, Finland Tel: +358 0 4747349.Fax: +358 0 4747497 E-mail: pirjo.turtianen@occupheath.fi Swedish Academy of Pharmaceutical Sciences, P.O. Box 1136, $111 8 1 Stockholm, Sweden Tel: +46 8 723 50 00. Fax: +46 8 20 55 11 Dr. R. Sniits, Royal Flemish Chemical Society (KVCV ), Working Party on Chromatography, BASF Antwerpen N.V., Central Laboratory, Haven 725, Scheldelaan 600, €3-2040 Antwerp, Belgium Tel: t32 3 561 2831. Fax: +32 3 561 3250 Spring Innovations, 18514 Moss Lane, Bramhall, Stockport, Cheshire. UK, SK7 IBD Tel: +44 @)I61 440 0082. Fax: +44 (01161 440 9127 The Pittsburgh Conference, 300 Penn Center Boulevard, Suite 332, Pittsburgh, PA 15235-5503, USA Cambridge Healthtech Institute, 1037 Chestnut Street, Newton Upper Falls.MA 02164, USA Tel: -+I 617 630 1300. Fax: +1 617 630 1325 E-mail: chi@ hea1thtech.comAnalyst, December 1995, Vol. 120 159N Date 10-15 19-23 20-2 1 24-28 25-29 3 1 4 4 April 9-10 9-12 9-12 17-19 22-23 23-26 28-1/5 May 5-8 Conference Location Advances in the Formulation and Processing of Injectable Dispersed Pharmaceuticals UK Cambridge, International Solvent Extraction Conference Melbourne, 1996 (ISEC '96) Australia External Sourcing of R & D (extRaD '96) Manchester, UK 29th International Meeting of the ESRDG of the RSC: ESR Spectroscopy of Inorganic Radicals and Metal Ions in Inorganic and Biological Systems ESEAC '96,6th European Conference on Elect roanal ysis UK Edinburgh, UK Durham, 7th International Symposium on Supercritical Indianapolis, Fluid Chromatography and Extraction USA 1996 Northeastern Environmental Symposium East Rutherford, 26th International Symposium on Environmental Analytical Chemistry Scanning '96 VIIth International Symposium on Luminescence Spectrometry in Biomedical Analysis-Detection Techniques and Applications in Chromatography and Capillary Electrophoresis Computer and Process Validation in the USA Vienna, Austria Monterey , USA Nice, France Manchester, Pharmaceutical and Fine Chemical Industries UK Analytica Conference '96 Munich, Germany 87th AOCS Annual Meeting and Expo Indianapolis, USA International Colloquium on Process Related Analytical Chemistry in Environmental Brazil Investigations Gramado, Contact Dr.J. A. Clements, Room 403, Royal Pharmaceutical Society of Great Britain, 1 Lambeth High Street, London, UK SE1 7JN Tel: +44 (0)171 735 9141.Fax: +44 (0)171 735 7629 Dr. R. W. Cattrall, Secretary Organising Committee, ISEC '96, School of Chemistry, La Trobe University, Rundoora 3083, Victoria, Australia Tel: +61 3 9479 2539. Fax: +61 3 9479 1399 E-mail: r.w.c.@latrobe.edu.au Spring Innovations, 185A Moss Lane, Bramhall, Stockport, Cheshire, UK SK7 1BA Tel: +44 (0)161 440 0082. Fax: +44 (0)161 440 9127 Dr. C. C. Rowlands, Department of Chemistry, University of Wales Cardiff, P.O. Box 912, Cardiff, UK CF13TB Dr. A. G. Fogg, Loughborough University of Technology, Loughborough, Leicestershire, UK LE113TU Tel: +44 (0) 1509 263171. Fax: +44 (0) 1509 233163 Mrs. Janet Cunningham, Ban Enterprises, 10120 Kelly Road, P.O. Box 279, Walkersville, MD 21793 USA Tel: +I 301 898 3772.Fax: +1 301 898 5596 Sandy Galla, ISC Exhibit Management Co., P.O. Box 313, Shelton. CT 06484-0313 Tel: +1 203 926 9300. Fax: +1 203 926 9722 Professor Dr. M. Grasserbauer, Institute for Analytical Chemistry, Vienna University of Technology, Getreidemarkt 9/15 1, A-1060 Wien, Austria Fax: +43 1 5867813 Mary K. Sullivan, Foundation for Advances in Medicine and Science, P.O. Box 832, Mahwah, NJ Tel: +I 201 818 1010. Fax: +1 201 818 0086 E-mail: fams@holonet.net Professor Willy R. G. Baeyens, University of Ghent, Pharmaceutical Institute, Department of Pharmaceutical Analysis, Harelbekestraat 72, B-9000 Ghent, Belgium Tel: +32 9 221 895 1. Fax: +32 9 221 4175 Spring Innovations, 185A Moss Lane, Bramhall, Stockport, Cheshire, UK SK7 1BA Tel: +44 (0)161 440 0082.Fax: +44 (0)161 440 9127 Congress Center, Messegelhde, D-80325 Miinchen, Germany Tel: +49 89 5107 159. Fax: +49 89 5107 180 AOCS Educationhleetings Department. P.O. Box 3489, Champaign, IL, USA 6 1826-3489 Tel: +1 217 359 2344. Fax: +I 217 351 8091 07430-0832, USA Centro de Ecologia, Universidade Federal do Rio Grande do Sul, C.P. 15007, 91501-970 Port0 Alegre, Brazil Tel: +55 51 2281 633. Fax: +55 51 3361 568. E-mail: Cenecaifl .ufrgs.Br160N Analyst, December 1995, Vol. 120 Date 6-8 6-10 9-1 1 13-14 19-22 19-24 20-22 20-23 20-24 23-25 June 9-1 3 10-1 1 10-14 13-14 16-21 Conference EuroResidue 111, Third International Conference on Residues of Veterinary Drugs in Food 2nd European Symposium and Exhibition on Photonics in Manufacturing I1 2nd Symposium on Biotechnology-From the Gene to Finished Product Chiral USA '96 4th International Symposium on Metal Ions in Biology and Medicine 9th International Symposium on Trace Elements in Man and Animals Symposium on Dairy Quality Assurance 2nd International Symposium & Workshop on Biological Environmental Specimen Banking (BESB 2) 18th International Symposium on Capillary Chromatography XIIIth National Conference on Analytical Chemistry 8th International Conference on Metalorganic Vapour Epitaxy 6th Conference on Total Reflection X-Ray Fluorescence Analysis and Related Methods (Part 1) Location Veldhoven, The Netherlands Paris, France Stockholm, Sweden Boston, USA Barcelona, Spain Banff, Canada Sonthofen, Germany Stockholm, Sweden Riva del Garda, Italy Craiova, Romania Cardiff, UK Eindhoven, Netherlands 11th International Converence on High-Power Prague, Particle Beams (BEAMS '96) Czech Republic 6th Conference on Total Reflection X-Ray Fluorescence Analysis and Related Methods (Part 2) Dortmund, Germany HPLC '96: 20th International Symposium on High Performance Liquid Phase Separations and Related Techniques California, USA Contact Dr.N. Haagsma, Utrecht University, Faculty of Veterinary Medicine, P.O. Box 80.175, NL-3508 TD Utrecht, The Netherlands Tel: +3 1 30 535365. Fax: +3 1 30 532365 Francoise Chavel, Executive, Secretary, European Optical Society, B.P. 147-91403 Orsay Cedex, France Tel: +33 1 69 85 35 92. Fax: +33 1 69 85 35 65. E-Mail: francoise.chavel@iota.u-psud.fr Swedish Academy of Pharmaceutical Sciences, P.O.Box 1136, S-1 1 1 81 Stockholm, Sweden Tel: +46 8 723 50 00. Fax: +46 8 20 55 11 Spring Innovations, 185A Moss Lane, Bramhall, Stockport, Cheshire, UK, SK7 1BD Tel: +44 (0) 16 1 440 0082. Fax: +44 (0) 16 1 440 9 127 Mercedes Gomez, Laboratory of Toxicology and Biochemistry, School of Medicine, c/o San Lorenzo 21, E-43201 Reus, Spain Tel: +34 77 759376. Fax: +34 77 759322 Mary L' Abbe, Nutrition Research, Health Canada, Ottawa, ON KIA OL2, Canada Tel: +1 613 957 0924. Fax: +1 613 941 6 182 E-mail:mlabbe@hpb.hwc.ca Michael Carl, Milschwirtschaffliche Untersuchungs und Versuchsanstalt Mempten, Postfach 2025, D874 10, Kempten, Germany Tel: +49 83 15 2900. Fax: +49 83 15 290100 BESB 2; Anita Moberg, Swedish Environmental Protection Agency, S- 10648 Stockholm, Sweden Tel: +46 8 698 1000.Fax: +46 8 689 1504. E-mail: amo@environ.se Professor D. P. Sandra, IOPMS, Kennedypark 20, B-8500 Kortrijk, Belgium Tel: +32 56 204960. Fax: +32 56 204859 Romanian Society of Analytical Chemistry, 13 Boulevard Republicii, Sector 3, 70346 Bucharest, Romania Tel: +40 1 631 00 60. Fax: +40 1 631 2279 Glenda Bland, Global Meeting Planning Tel: +44 (0)1222 700053. Fax: +44 (0)1222 700665 E-mail: 10046. l402@compuserve.com Dr. D. K. G. de Boer, Philips Research Laboratories, WB21, Prof. Holstlaan 4, NL-5656 AA Eindhoven, The Netherlands Tel: +3 1 40 74 2859. Fax: +3 1 40 74 3075. E-mail: deboerd@ prl.philips .nl Dr. Jiri Ullschmied, Conference Co-Chairman, Institute of Plasma Physics, AS CR, Za Slovankou 3, Prague 182 00, Czech Republic Fax: +422 858 6389.E-Mail: BEAMS96@IPP.CAS.CZ Dr. D. K. G. de Boer, Philips Laboratories WB2 1, Prof. Holstlaan 4, NL-5656 AA Eindhoven, The Netherlands Tel: +31 40 74 2859. Fax: +31 40 74 3075. E-mail: deboerd@prl.philips.nl Mrs. Janet Cunningham, Barr Enterprises, 10120 Kelly Road, P.O. Box 279, Walkersville, MD 21793, USA Tel: +1 301 898 3772. Fax: +1 301 898 5596Analyst, December 1995, Vol. 120 161N Date 1 7-2 1 30-517 July 1-3 8-1 2 17-19 Conference 2nd European Symposium and Exhibition on Optical Instrument and Systems Design Resonance Ionization Spectroscopy and Its Applications, RIS-96 9th International Symposium on Polymer Analysis and Characterization (ISPAC-9) XVI International Congress of Clinical Chemistry 8th Biennial National Atomic Spectroscopy Symposium (BNASS) August 11-16 20-23 7th International Symposium on ICORS '96: XV International Conference on Raman Spectroscopy Pharmaceutical and Biomedical Analysis (PBAT '96) 25-30 XXIII EUCMOS September 1-7 Euroanalysis IX 8-13 CLEO '96: European Conferences on Lasers and Electro-Optics 9-1 1 Sixth International Symposium on Field Flow Fractionation 9-13 14th International Conference on High Resolution Molecular Spectroscopy 10-14 International Symposium and Exhibition on Biomedical Optics IV Location Glasgow, UK Pennsylvania, USA Oxford, UK London, UK Norwich, UK Pittsburgh, USA Osaka, Japan Balatonfured, Hungary Bologna, Italy Hamburg, Germany Ferrara, Italy Prague, Czech Republic Graz, Austria Contact Francoise Chavel, Executive Secretary, European Optical Society, B.P.147-91403 Orsay Cedex, France Tel: +33 1 69 85 35 92. Fax: +33 1 69 85 35 65. E-Mail: francoise.chavel@iota.u-psud.fr Sabrina Glasgow, Conference Secretary, Department of Chemistry, The Pennsylvania State University, I84 Materials Research Institute Building, University Park, PA 16802-7003 USA Tel: +1 814 865 0200. Fax: +1 814 863 0618 E-mail: scg@psuvm.psu.edu Prof. John Dawkins, Department of Chemistry, Loughborough University of Technology, Loughborough, Leicestershire, UK LE11 3TU Fax: +44 (0)1509 233163 Mrs. Pat Nielsen, XVIth International Congress of Clinical Chemistry, P.O. Box 227, Buckingham, UK MK18 5PN Fax: +44 (0) 1280 6487 Ms. Brenda Holliday, BNASS Secretariat, Royal Society of Chemistry, Thomas Graham House, Science Park, Milton Road, Cambridge, UK CB4 4WF Tel: +44 (0)1223 420066.Fax: +44 (0)1223 423623 Professor S. Asher, Department of Chemistry, University of Pittsburgh, Pittsburgh, PA 15260, USA Professor Susumu Honda, Faculty of Pharmaceutical Sciences, Kinki University, Kowakae 3-4- 1 , Higashi Osaka 577, Japan Fax: +81 6 721 2353 Professor Dr. J. Mink, Department of Analytical Chemistry, University of VeszprCm, P.O. Box 158, H-8201 Veszprkm, Hungary Professor Luigia Sabbatini, Euroanalysis IX, Dipartimento di Chimica, Universiti di Bari, Via Orabona, 4, 70126 Bari, Italy Tel: +39 80 544020. Fax: +39 80 544026 CLEO/Europe '96, Institute of Physics, Meetings and Conferences Department, 47 Belgrave Square, London, UK SW 1X 8QX F. Dondi, Department of Chemistry, University of Ferrara, Via L.Borsari, 46, 1-44100 Ferrara, Italy Tel: +39 532 291 154. Fax: +39 532 240709 Dr. V. Spirko, Academy of Sciences of the Czech Republic, J. Heyrovsk, Institute of Physical Chemistry, Dolejskova 3, (22-18223 Praha 8, Czech Republic Francoise Chavel, Executive Secretary, European Optical Society, B.P. 147-91403 Orsay Cedex, France Tel: +33 1 69 85 35 92. Fax: +33 1 69 85 35 65. E-Mail: francoise.chavel@iota.u-psud.fr162N Analyst, December 1995, Vol. 120 Date Conference 11 22nd Annual Meeting of the British Mass Spectrometry Society 15-20 21st International Symposium on Chromatography 16-1 8 The Third International Conference on Applications of Magnetic Resonance in Food Science November 4-8 1997 April 14-19 May 12-16 June 15-2 1 16-20 30-317 International Symposium on the Industrial Application of the Mossbauer Effect Genes and Gene Families in Medical, Agricultural and Biological Research: 9th International Congress on Isozymcs European Symposium on Photonics in Manufacturing 111 International Conference on Analytical Chemistry European Symposium on Environmental and Public Safety I1 6th European ISSX Meeting September 8-12 Biomedical Optics V Location Swansea, UK Stuttgart, Germany Nantes, France Johannesburg, South Africa Texas, USA Paris, France Moscow, Russia Munich, Germany Gothenburg, Sweden Poland Contact Dr.Fred Mellon, Institute of Food Research, Norwich Laboratory, Norwich Research Park, Colney, Norwich, UK NR4 7UA Tel: +44 (0)1603 255299. Fax: +44 (0)1603 452578 E-mail : fred.mellon@ bbsrc.ac .uk GDCh-Geschaftsstelle, Abt. Tagungen, Varrentrappestr. 40-42, Postfach 90 04 40, D-6000 Frankfurt am Main 90, Germany Tel: +49 69 791 7358. Fax: +49 69 791 7475 G. J. Martin or V. Foucault, FacultC des Sciences, Laboratoire de Resonance Magnetique NuclCaire et RCactivitiC Chimique, U.R.A. - CNRS 472, 2 rue de la Houssinikre, 44072 Nantes Cedex 03, France Tel: +33 4037 3169. Fax: +33 4074 9806 Herman Pollak, Mossbauer Laboratory, University of the Witwatersrand, Private Bag 3, WITS 2050, Johannesburg, South Africa Tel: +27 11 716 4053/2526. Fax: +27 11 339 8262. E-Mail: ISIAME@PHY SNET.PHY S .WITS.AC.ZA Mrs. Janet Cunningham, Barr Enterprises, 10120 Kelly Road, P.O. Box 279, Walkersville, MD 21793, USA Tel: +1 301 898 3772. Fax: + I 301 898 5596 Francoise Chavel, Executive Secretary, European Optical Society, B.P. 147-91403 Orsay Cedex, France Tel: +33 1 69 85 35 92. Fax: +33 1 69 85 35 65. E-Mail: francoise.chavel@iota.u-psud.fr Dr. L. N. Kolomiets, Scientjfic Council on Chromatography of the Russian Academy of Sciences Leninsky Prospect 31, 117915 Moscow, Russia Fax: +7 095 952 0065 Francoise Chavel, Executive, Secretary, European Optical Society, B.P. 147-91403 Orsay Cedex, France Tel: +33 1 69 85 35 92. Fax: +33 1 69 85 35 65. E-Mail: francoise.chavel@iota.u-psud.fr Meeting Secretariat, 6th European ISSX Meeting, c/o The Swedish Academy of Pharmaceutical Sciences, P.O. Box 1136, S-111 81 Stockholm, Sweden Tel: +46 8 723 5000. Fax: +46 8 20 55 11 Francoise Chavel, Executive Secretary, European Optical Society, B.P. 147-91403 Orsay Cedex, France Tel: +33 1 69 85 35 92. Fax: +33 1 69 85 35 65. E-Mail: francoise.chavel@iota.u-psud.fr

ISSN:0003-2654    

DOI:10.1039/AN995200158N

出版商:RSC    

年代:1995

数据来源: RSC

摘要:

Analyst, Decmzher 1995, Vol. 120 163N Courses Date Conference Location 1996 January 8-9 Present Status of Analysis of Trace Metals Trivandrum, and Nutrients in the Environment India 24-26 Validation in Pharmaceutical Analysis York, UK February 5-6 5-6 5-6 5-6 5-6 6-8 The Next Step in Capillary Gas Chromatography for Trace Analysis Belgium Bruges, Pre- and Postcolumn Techniques in HPLC for Bruges, Improved Analyte Isolation, Derivatization, Belgium Clean-up, Separation and Detection Isotopically Labelled Compounds in Bruges, Hyphenated GC-techniques Belgium Analytical Tools for GC-MS (Advanced Modes of Ion-trap Mass Spectrometry) Bruges, Belgium Biomedical Applications of GC-MS Bruges, Belgium HPLC Beginners Training Course Macclesfield, UK 12-14 Package Testing of Pharmaceuticals Cobham, UK March 26 Intermediate HPLC Training Course 27 Intermediate HPLC Training Course 28 Intermediate HPLC Training Course April 23-24 HPLC Troubleshooting Courses Macclesfield, UK Maccles field, UK Macclesfield, UK Macclesfield, UK Contact Dr.C. S. P. Iyer, Convener, ICES-96, Regional Research Laboratory (CSIR), Trivandrum 695 0 19, India Tel: +91 471 77459. Fax: +91 471 75186. E-mail: rrlt@ sirnetm.ernet.in Dr. J. A. Clements, Room 403, Royal Pharmaceutical Society of Great Britain, 1 Lambeth High Street, London SEl 7JN Tel: +44 (0) 17 1 735 9 145. Fax: +44 (0) 17 1 735 7629 Congress Secretariat, Ordibo bvba, L. Hennincksraat 18, B-2610 Wilri.jk, Antwerpen, Belgium Tel: +32 38 28 89 61. Congress Secretariat, Ordibo bvba, L. Hennickstraat 18, B-26 10 Wilrijk, Antwerpen.Belgium Tel: +32 38 28 89 61. Congress Secretariat, Ordibo bvba, L. Henninckstraat 18, B-26 10 Wilrijk, Antwerpen, Belgium Tel: + 32 38 28 89 6 1. Congress Secretariat, Ordibo bvba. L. Henninckstraat 18, B-26 10 Wilrijk, Antwerpen, Belgium Tel: 1-32 38 28 89 61. Congress Secretariat, Ordibo bvba, L. Henninckstraat 18, B-26 10 Wilrijk, Antwerpen, Belgium Tel: + 32 38 28 89 61. Nikki Rathbone, HPLC Technology Ltd, Macclesfield, Cheshire, UK, SK 1 1 6PJ Tel: 01625 613848. Fax: 01625 616916 Dr. J. A. Clements, Room 403, Royal Pharmaceutical Society of Great Britain, 1 Lambeth High Street, London SEI 7JN Tel: +44 (0)171 735 9145. Fax: +44 (0)171 735 7629 Nikki Rathbone, HPLC Technology Ltd, Macclesfield, Cheshire, UK SK 1 1 6PJ Tel: 01625 613848. Fax: 01625 616916 Nikki Rathbone, HPLC Technology Ltd, Macclesfield, Cheshire, UK SKI 1 6PJ Tel: 01625 613848. Fax: 01625 616916 Nikki Rathbone, HPLC Technology Ltd, Macclesfield, Cheshire, UK SKI 1 6PJ Tel: 0 1625 6 13848. Fax: 0 1625 6 169 16 Nikki Rathbone, HPLC Technology Ltd, Macclesfield, Cheshire, UK SKI 1 6PJ Tel: 01625 613848. Fax: 01625 616916 Entries in the above listing are included at the discretion of the Editor and are free of charge. If you wish to publicize a forthcoming meeting please send full details to: The Analyst Editorial Office, Thomas Graham House, Science Park, Milton Road, Cambridge, UK CB4 4WF. Tel: +44 (0) 1223 420066. Fax: +44 (0) 1223 420247. E-mail:Analyst@RSC.ORG.

ISSN:0003-2654    

DOI:10.1039/AN995200163N

出版商:RSC    

年代:1995

数据来源: RSC

摘要:

164N Analyst, December 1995, Vol. 120 ~ Recent IUPAC Recommendations IUPAC Draft: Reauest for Public Comment infrared spectral regions. Raman scattering can be divided into linear andnon-linear processes. Because oT their importance for Raman effects. The has been made for Public chemical analysis, the treatment is confined mainly to the linear review. Laser-based Molecular Spectroscopy for Chemical Analysis-Raman Scattering Processes Copies of the text may be obtained from Dr Alan McNaught, The Royal Society of Chemistry, Thomas Graham House, This report is the 18th in a series on Spectrochemical Methods of Analysis. It is concerned with Raman scattering processes, usually induced by lasers, covering the UV, visible, and near- Science-Park, Miiton Road, Cambridge CB4 4WF. IUPAC would welcome comments (by 31 May 1996) before prepara- tion of a final draft for publication in Pure Appl. Chem.

ISSN:0003-2654    

DOI:10.1039/AN995200164N

出版商:RSC    

年代:1995

数据来源: RSC

摘要:

165N Analyst, December 1995, Vol. 120 Future Issues Will lnclude- Application of Near Infared Reflectance Spectrometry to the Analytical Control of Pharmaceuticals: Ranitidine Hydro- chloride Tablet Production-Piero Corti, Elena Dreassi, Giuseppe Ceramelli, Luisa Savini, Piero Luigi Perruccio and Silvano Lonardi Determination of Cinnamic Acid in Human Urine by Differ- ential-pulse Polarography-Maria Valnice B. Zanoni, Valdir S. Ferreira, Cristo B. Melios and Nelson R. Stradiotto Antimony Speciation in Freshwater Plant Extracts by Using Hydride Generation-Gas Chromatography-Mass Spectro- metry-Matthew Dodd, Spiros A. Pergantis, William R. Cullen, Hao Li, Guenter K. Eigendorf and Kenneth J. Reimer Rotary and Continuous Extraction of Phenolic Acids and Aldehydes from Wine-J. A.Perez-Bustamante, E. R. Bru, C. G. Barroso and R. Cela Distribution of Selenium in Human Blood Plasma and Serum- I. Harrison, David Littlejohn and G. s. Fell Gel Permeation Chromatography in the Detection of Veterinary Drugs in Foodstuffs: Sulfonamides, Nitrofurans, Carbadox, Olaquindox-R. Angeletti, G. Biancotto and R. Piro Rapid and Reliable Method for the Determination of Alumin- ium in Bone by Electrothermal Atomic Absorption Spectro- metry-Patrick J. Parsons, Shida Tang and Walter Slavin Towards the Characterization of Bitumen-Mineral Interactions in a Natural Asphalt-Clayton Smith, Lutchminarine Chatergoon and Robin Whiting Methods for the Analysis of Beta-agonists in Biological Matrices-Michael O’Keeffe, Damien Boyd and Malcolm R. Smyth Measurement of Carbon- 13 : Carbon- 12 ratios by Fourier Trans- form Infrared Spectrometry-Iain L. Marr and A.Kindness Determination of Alkylphenol Ethoxylate Non-ionic Surfac- tants in Trade Effluents by Sublation and High-performance Liquid Chromatography-B. B. Wheals and Naaim M. A. Ibrahim Electrochemical Activation of Screen-printed Carbon Strips- Joseph Wang, Maria Pedrero, Henning Sakslund, Ole Hammerich and Jose M. Pingarron Direct Determination of 7-Hydroxycoumarin and 7-Hydrox- ycoumarin-glucuronide, in urine and plasma, by capillary electrophoresis-Richard O’Kennedy, Declan Bogan, R. D. Thorens, E. A. Schafer and M. Tegtmeier Colloidal Gold Supported onto Glassy Carbon Substrates as Amperometric Sensor for Carbohydrates in Flow-injection Analysis and Liquid Chromatography-Innocenzo G.Casella, Angelo Destradis and Elio Desimoni Pretreatment of Microelectrodes: Comparison of Polishing Procedures by Statistical Analysis of Voltammetric Data- Terence J. Cardwell, Alan M. Bond, Jan Mocak and Jose H. Santos Fluorescence Optical Sensor for Low Concentrations of Dissolved Carbon Dioxide-Beat Muller and Peter C. Hauser Development of a Stand-alone Affinity Clean-up for LSD in Urine-John M. Francis and Derek H. Craston Precedures and Problems in the Determination of a Suite of Elements in Human Femoral Bone Using Inductively Coupled Plasma Atomic Emission Spectrometry and Inductively Coupled Plasma Mass Spectrometry-Norman B. Roberts, H. P. J. Walsh, T. R. Helliwell, S. A. Kelly, L. Klenerman, J. Haines and R. Clark Preconcentration and Determination of Some Lanthanide Elements with Immobilized Bacteria by Flow Injection In- ductively Coupled Plasma Atomic Emission Spectrometry- Angel Maquieira, Hayat Elmahadi and Rosa Puchades On-line Separation and Sequential Determination of Trace Heavy Metals in Biological Materials by Flow Injection Inductively Coupled Plasma Atomic Emission Spectrometry- M.T. Siles Cordero, E. Vereda Alonso, Amparo Garcia de Torres and Jose Manuel Can0 Pavon Direct Determination of Lead in Gasoline Using Emulsification and Argon and Argon-Oxygen Inductively Coupled Plasma Mass Spectrometry-I. B. Brenner, A. T. Zander, S. Kim and J. Shkolnik Direct On-line Microwave-assisted Digestion of Shellfish Tissue for the Determination of Selenium-Marco A. Z. Arruda, Mercedes Gallego and Miguel Valcarcel Determination of Atmospheric Trace Metal Concentrations by Isotope Dilution Inductively Coupled Plasma Mass Spectro- metry-Kunihiko Akatsuka, Takunori Katoh, Masayuki Akiyama, Hideyuki Ohtsuka, Seiji Nakamura and Kensaku Haraguchi Evaluation of a Low Sample Consumption, High-efficiency Nebulizer for Elemental Analysis of Biological Samples Using Inductively Coupled Plasma Mass Spectrometry-Huiying Liu, Scott P.Dolan, Robert S. Schwartz and Akbar Montaser Accurate and Precise Measurements of Lead in Bone Using Graphite Furnace Atomic Absorption Spectrometry with Zee- man-effect Background Correction-Yan Y. Zong, Patrick J. Parsons and W. Slavin COPIES OF CITED ARTICLES The Royal Society of Chemistry Library can usually supply copies of cited articles. For further details contact: The Library, Royal Society of Chemistry, Burlington House, Piccadilly, London WlV OBN, UK. Tel: +44 (0)171-437 8656. Fax: +44 (0) 17 1-287 9798. Telecom Gold 84: BUR2 10. Electronic Mailbox (Internet) LIBRARY@RSC.ORG. If the material is not available from the Society’s Library, the staff will be pleased to advise on its availability from other sources. Please note that copies are not available from the RSC at Thomas Graham House, Cambridge.

ISSN:0003-2654    

DOI:10.1039/AN995200165N

出版商:RSC    

年代:1995

数据来源: RSC

摘要:

Technical Abbreviations and Acronyms The presence of an abbreviation or acronym in this list should NOT be read as a recommendation for its use. However, those defined here need not be defined in the text of your manuscript. AAS ac AID ADC ANOVA AOAC ASTM bP BSA BSI CEN CPm CMOS c.m.c. CRM CVAAS C.W. CZE dc DRIFT dPm DELFIA DNA EDTA ELISA emf ETAAS EXAFS EPA FAAS FAB FAO-WHO FIR FT FPLC FPD GC GLC HGAAS HPLC ICP id INAA IR ISFET iv im IGFET ISE LC LED LOD atomic absorption spectrometry alternating current analogue-to-digital analogue-to-digital converter analysis of variance Association of Official Analytical Chemists American Society for Testing and Materials boiling point bovine serum albumin British Standards Institution European Committee for Standardization counts per minute complementary metal oxide silicon critical micellization concentration certified reference material cold vapour atomic absorption spectrometry continuous wave capillary zone electrophoresis direct current disintegrations per minute diffuse reflectance infrared Fourier transform spectroscopy dissociation enhanced lanthanide fluorescence immunoassay deoxyribonucleic acid ethylenediamine t et raace tic acid enzyme linked immunosorbent electromotive force electrothermal atomic absorption spectrometry extended X-ray absorption fine structure spectroscopy Environmental Protection Agency flame atomic absorption fast atom bombardment Food and Agriculture Organization, far-infrared Fourier transform fast protein liquid chromatography flame photometric detector gas chromatography gas-liquid chromatography hydride generation atomic absorption spectroscopy high-performance liquid chromatography inductively coupled plasma internal diameter instrumental neutron activation infrared ion-selective field effect transistor intravenous intramuscular insulated gate field effect transistor ion-selective electrode liquid chromatography light emitting diode limit of determination assay spectrometry World Health Organization analysis LOQ mP MRL mRNA MS NIR NMR NIST od OES PBS PCB PAH PGE PIXE PPt PPb PPm PTFE PVC PDVB QC QA REE rf RIMS rms 'pm RNA SCE SE SEM SIMS SIMCA SRM STM STP TIMS TLC TOF TGA TMS tris TRIS uv UVNIS VDU XRD XRF YAG Commonly Used Symbols A4 Mr r S U limit of quantification melting point maximum residue limit messenger ribonucleic acid mass spectrometry near-infrared nuclear magnetic resonance National Institute of Standards and Technology outer diameter optical emission spectrometry phosphate buffered saline polychlorinated biphenyl polycyclic aromatic hydrocarbon platinum group element particle/proton-induced X-ray parts per trillion (1012; pg g-l) parts per billion (109; ng g-l) parts per million (106; pg g- ) poly(tetrafluoroethy1ene) poly(viny1 chloride) poly( divinyl benzene) quality control quality assurance rare earth element radiofrequency resonance-ionization mass spectrometry root mean square revolutions per minute ribonucleic acid saturated calomel (reference) electrode standard error scanninglsurface (reflection) secondary-ion mass spectrometry soft independent modelling of class Standard Reference Material scanning tunnelling (electron) standard temperature and pressure thermal ionization mass thin-layer chromatography time-of-flight thermogravimetric analysis trimethylsilane 2- amino-2-( hy droxyme t hy1)- propane-173-diol (ligand) 2-amino-2-( hydroxymethy1)- propane-l,3-diol (reagent) ultraviolet ultraviolet-visible visual display unit X-ray diffraction X-ray fluorescence yttrium aluminium garnet emission electron microscopy analogy microscopy spectrometry molecular mass relative molecular mass correlation coefficient standard deviation atomic mass

ISSN:0003-2654    

DOI:10.1039/AN995200166N

出版商:RSC    

年代:1995

数据来源: RSC